One-Pot o-Nitrobenzenesulfonylhydrazide (NBSH) Formation-Diimide Alkene Reduction Protocol
Reference:
Marsh, B. J. and Carbery, D. R., 2009. One-Pot o-Nitrobenzenesulfonylhydrazide (NBSH) Formation-Diimide Alkene Reduction Protocol. Journal of Organic Chemistry, 74 (8), pp. 3186-3188.
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Official URL:
http://dx.doi.org/10.1021/jo900237y
Abstract
A one-pot protocol for the formation of 2-nitrobenzenesulfo-nylhydrazide (NBSH) from commercial reagents and subsequent alkene reduction is presented. The transformation is operationally simple and generally efficient for effecting diimide alkene reductions. A range of 16 substrates have been reduced, highlighting the unique chemoselectivity of diimide as a reduction system.
Details
| Item Type | Articles |
| Creators | Marsh, B. J.and Carbery, D. R. |
| DOI | 10.1021/jo900237y |
| Departments | Faculty of Science > Chemistry |
| Refereed | Yes |
| Status | Published |
| ID Code | 14193 |
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