Marsh, B. J. and Carbery, D. R., 2009. One-Pot o-Nitrobenzenesulfonylhydrazide (NBSH) Formation-Diimide Alkene Reduction Protocol. Journal of Organic Chemistry, 74 (8), pp. 3186-3188.
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A one-pot protocol for the formation of 2-nitrobenzenesulfo-nylhydrazide (NBSH) from commercial reagents and subsequent alkene reduction is presented. The transformation is operationally simple and generally efficient for effecting diimide alkene reductions. A range of 16 substrates have been reduced, highlighting the unique chemoselectivity of diimide as a reduction system.
|Item Type ||Articles|
|Creators||Marsh, B. J.and Carbery, D. R.|
|Departments||Faculty of Science > Chemistry|
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