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The synthesis and characterisation of C-triorganometallated (metal = Sn, Si) bis-(thienyl)- and bis-(pyrazolyl)alkanes, including the crystal structure of [(Ph3Sn)C3N2](2)CH2


Reference:

Hill, M. S., Mahon, M. F., McGinley, J. M. G. and Molloy, K. C., 2001. The synthesis and characterisation of C-triorganometallated (metal = Sn, Si) bis-(thienyl)- and bis-(pyrazolyl)alkanes, including the crystal structure of [(Ph3Sn)C3N2](2)CH2. Polyhedron, 20 (15-16), pp. 1995-2002.

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Abstract

C-organostannyl- and organosilyl-derivatives of 2-(thien-2-ylmethyl)thiophene and 1-[(1H-pyrazol-1-yl)methyl]-1H-pyrazole have been synthesised and characterised spectroscopically. Lithiation and subsequent substitution by R3M takes place at the 5,5' positions for both bis-heterocycles, and this is confirmed by the X-ray structure of 1,1'-[5,5'-(Ph3Sn)C3N2](2)CH2. (C) 2001 Elsevier Science Ltd. All rights reserved.

Details

Item Type Articles
CreatorsHill, M. S., Mahon, M. F., McGinley, J. M. G. and Molloy, K. C.
DepartmentsFaculty of Science > Chemistry
RefereedYes
StatusPublished
ID Code5214
Additional InformationID number: ISI:000169986500030

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